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Technical

How bentonite is tested, and what the numbers mean

Written for the engineer who specifies the purchase, not only the buyer who places it.

Test methods

What each test actually measures

Swell index

ASTM D5890

Two grams of dry clay is sprinkled into 100 mL of water and left to settle. The settled volume in millilitres is the swell index, the most quoted number in the bentonite trade.

API filtrate

API 13B-1

A mud sample is held at 100 psi against filter paper for 30 minutes. Low filtrate means a thin, tight filter cake that stops fluid escaping into the formation.

Viscometer readings

API 13B-1

A rotational viscometer reads the mud at 600 and 300 r/min. From these come apparent viscosity, plastic viscosity and yield point.

Marsh funnel viscosity

Marsh funnel

The time for 946 mL of slurry to drain from a standard funnel. The quickest site check for piling and HDD slurry.

Methylene blue

MB titration

Methylene blue dye is titrated into a slurry until the clay adsorbs no more. It measures how much active clay you are actually buying.

Enslin water absorption

Enslin-Neff

How much water the clay draws up over time. Pellet plants use it to compare binders at equal dosage.

Green compression strength

AFS

A rammed sand specimen is crushed and the peak load recorded. It decides whether a mould holds its shape. Foundries buy this number.

Residue on 75 µm

Wet sieve

Grit left on a 200-mesh sieve after washing. Above 2.5% a clay fails OCMA grade, and grit wears pumps and mixers.

For what the standards require, see API 13A and OCMA explained.

Geology

Where Kutch bentonite comes from

Bentonite in Kutch (Kachchh) is a weathering product of Deccan Trap basalt, formed in the Palaeocene, roughly 65 to 58 million years ago. Bentonite, white clay and laterite are levels of the same weathering profile.

Soiloverburden
Lateriteiron-rich cap
Kaolinitic white clayplastic, non-swelling
Bentonitemontmorillonite, swelling
Weathered basalt—
Deccan Trap basaltbasement

Where drainage was poor, silica stayed in place and montmorillonite formed: that is bentonite. Where drainage was efficient, silica was flushed out and the clay became kaolinitic: the kind of deposit our plastic white clay comes from. Further leaching leaves laterite.

The ore bodies are lenses and pockets a few metres thick, not continuous seams. Clay changes from lens to lens, which is why we keep faces separate, stockpile by grade and test every lot rather than every season.

Why activation matters here. Kutch bentonite is mostly calcium-rich. Soda ash swaps that calcium for sodium so the clay swells and gels. It only works on montmorillonite, so it is a reason to test the raw clay, not a way round it.
A shallow pit exposing pale kaolinitic white clay beneath brown soil in Kutch
Pale kaolinitic clay exposed under the soil, Kutch

Test it against what you buy today.

A 2.5 kg sample with its certificate of analysis, sent by DHL or FedEx. Tell us your current supplier's figures and we will tell you honestly how ours compare.

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