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Technical reference

There is no Grade A bentonite.

Bentonite has no single quality ladder. There are industry standards, and a grade simply means the clay meets one industry’s specification. API and OCMA are two of those, and both belong to drilling.

01

What API and OCMA actually are

API

American Petroleum Institute

The document is API Specification 13A, “Drilling Fluids Materials”. It covers everything that goes into drilling mud: barite, bentonite, attapulgite, sepiolite, starch and more. Bentonite is tested on a suspension of 22.5 g in 350 cm³ of water, by the methods in API 13B-1.

ISO 13500 is the international equivalent and follows API 13A closely.

OCMA

Oil Companies Materials Association

A British body that wrote materials specifications for the North Sea oil industry. Its bentonite specification was designated DFCP-4.

OCMA no longer exists, but its specification lives on inside API 13A as OCMA-grade bentonite: Section 19 in the current 19th edition, Section 11 in earlier editions.

A buyer asking for “OCMA grade” today is asking for the OCMA-grade section of API 13A.

02

Section 9 against OCMA-grade

The two bentonite specifications most export buyers ask for, side by side. Read it carefully: one is not simply better than the other.

PropertyTest methodSection 9
Bentonite
OCMA-grade
bentonite
Viscometer dial reading at 600 r/minAPI 13B-1min 30min 30
Yield point / plastic viscosity ratioAPI 13B-1max 3max 6
Filtrate volume, 30 minAPI 13B-1max 15.0 cm³max 16.0 cm³
Residue greater than 75 µmWet sievemax 4.0%max 2.5%
MoistureOven drymax 10%not specified
Not a ranking. Section 9 is stricter on yield point ratio and filtrate. OCMA-grade is stricter on grit, 2.5% against 4.0%. They are two envelopes for two kinds of buyer. API 13A also has a separate section for non-treated bentonite, tested in a dispersed condition, which soda-activated clay cannot claim.
Section 9

Who asks for it

Oilfield mud companies that want the most viscosity per tonne and specify by the API section number.

OCMA-grade

Who asks for it

Water-well, HDD and many Gulf and African drilling buyers. The most traded drilling bentonite grade out of India.

Where our drilling lots sit against those limits

PROPERTYPasses the standardAPI 13A limitOur typical, OCMA (OCM)Section 9 (DRL)Viscometer dial at 600 r/minHigher is better30OCM 3330DRL 32Yield point / plastic viscosityLower is better6OCM 4.13DRL 2.5Filtrate, 30 minLower is better16 cm³OCM 14.615 cm³DRL 13.9Residue > 75 µmLower is better2.5%OCM 1.94%DRL 2.4

Our two drilling lots, OCM and DRL, are specified against these two columns. See the drilling grade specification.

03

“API grade” and the API Monogram are different things

Anyone can write “API grade” on a bag. Only a licensee may print the API Monogram, and that licence needs an API Spec Q1 quality system and an on-site audit by API.

We supply to the API 13A specification with an independent certificate of analysis for every shipment. We do not hold the Monogram, and we do not print it.

What backs each claim

ClaimWhat backs it
“API grade”, no certificateThe seller’s word
Certificate from an independent accredited labAn independent test
Pre-shipment inspection (SGS, BV, Intertek)A witnessed sample
API MonogramAn audited system
04

How bentonite is classified

A
Natural sodium bentonite Sodium is the dominant exchangeable cation. Swells strongly and builds viscosity. Wyoming is the benchmark.
B
Calcium bentonite Calcium dominant, swells far less. Most Indian deposits, Kutch included, are calcium or calcium-magnesium bentonite.
C
Soda-activated bentonite Calcium bentonite treated with soda ash, which swaps calcium for sodium so the clay swells and gels. Standard practice in Kutch and accepted by API 13A. This is what we sell.
D
Acid-activated bentonite (bleaching earth) Leached with acid to open up surface area, for decolourising edible and mineral oils. A different product.
E
Organoclay Bentonite treated with quaternary ammonium compounds so it disperses in oil. Used in paints, greases and oil-based mud.
The distinction that catches people out. Soda-activated bentonite is not natural sodium bentonite and should never be sold as such. A technical buyer can tell the difference, and a supplier caught blurring it loses the account.
05

Every industry, and the standard that governs it

ApplicationGoverning standardThe numbers that decide it
Drilling fluidsAPI Spec 13A (Section 9, OCMA-grade)
ISO 13500
600 r/min dial reading, YP/PV ratio, filtrate, residue
Piling, diaphragm walls, tunnellingEN 1538, EN 1536
Project specification
Density, Marsh funnel viscosity, fluid loss, pH, sand content
Foundry green sandAFS test methods
IS 12446
Green and dry compression strength, active clay, fineness
Iron ore pelletisingNo standardSwell index, Enslin water absorption, methylene blue index
Geosynthetic clay linersASTM D5890, ASTM D5891Swell index and fluid loss
Cat litterNo standardClump strength, absorption, dust
Ceramic bodiesNo standardPlasticity, dry strength, fired colour, shrinkage
Two sales processes. Where a written standard exists, a certificate opens the door. Where none does, the order is won by sending a sample and beating the current supplier in a side-by-side trial.
06

Two mistakes that cost buyers money

Mistake 1

Buying “Grade A”

Grade A, Grade 1, Premium and Super are seller labels with no meaning outside that seller’s office. Ask for the standard, or the test method and the value: “swell index 24 mL/2 g by ASTM D5890”.

Mistake 2

Buying one number instead of a range

A single good result shows one good lot. A published guaranteed range, with a certificate for every shipment, shows a supplier willing to be held to it.

Check the edition. API renumbers sections between editions. OCMA-grade bentonite moved from Section 11 to Section 19 in the 19th edition. If a datasheet quotes a section number, check which edition it refers to.

Test it against what you buy today.

A 2.5 kg sample with its certificate of analysis, sent by DHL or FedEx. Tell us your current supplier's figures and we will tell you honestly how ours compare.

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